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Polymer reagents, catalysts, and substrates have practical advantages compared to their small molecule analogs An insoluble polymer reagent, catalyst, or substrate can be easily separated from the other (ie, the small molecule) components of a reaction system by ltration This ease of separation allows the synthesis of high-purity products and the recovery of the polymeric species, with resulting economies Reactions with functional polymers are sometimes advantageously carried out in a manner similar to that for column chromatography The polymeric species is packed in a column and the small molecule species poured through the column Some of the more speci c details are described in Secs 9-12 through 9-14 When the polymer reagent, catalyst, or substrate is easily recoverable, it can be economically used in large excess to achieve high yields in a reaction.

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On my human voice synthesizers, I use a rotary switch to choose among crystals so that the voices can speak from bass to tenor, and then some (see 11). If you re into the idea of extending the frequency range of your DH 100, see Figure 31-4 for a super-simple crystal switcher. The crystals can be soldered to the rotary switch poles and chosen with the turn of a dial. All you need to do is to clip (or de-solder) the original crystal from the DH 100 board and replace it with the switch/crystal circuit as shown. Experiment with crystals both above and below the original 12.0 MHz. Canned crystals are okay to use instead of the ceramic original; such are available through Radio Shack in frequencies from 1.8432 MHz (part number 900-5089) to 20 MHz (part number 900-5126). These once-common items are no longer shelved at Radio Shack and will probably need to be special ordered or found elsewhere. Try to incorporate a series of crystals that will provide you with a nice frequency range to work with, lowest to highest.

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Small-molecule reagents, catalysts, or substrates that are highly reactive, toxic, or malodorous can be handled much more safely and easily in the form of the corresponding polymers Other advantages of functional polymers may arise from the enhancement of rate or equilibrium due to factors discussed in Sec 9-1 These factors may also lead to negative effects in some systems There are disadvantages that limit the commercial utilization of polymer reagents, catalysts, and substrates at this time Functional polymers are more expensive than their smallmolecule analogs Many applications that work well in the laboratory fail the economics of industrial use One needs large-scale uses where one or another of the advantages of functional polymers cannot be achieved by other means Filtration of a polymer reagent, catalyst, or substrate is often not easy.

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Fine particles slough off from larger beads or ground resin because of the stresses resulting from mechanical stirring or shaking These nes interfere with ltration by clogging the lters For a few functional polymers, the functional group(s) of importance may not be permanently anchored; in other words, the functionalization reaction is reversible This is the case with some polymer catalysts containing transition metal groups The transition metal components leach out with time Organic supports are of lesser stability than inorganic supports The advantages of functional polymers are best realized when used in two situations multistep sequential reactions and automated parallel combinatorial synthesis to produce libraries of compounds In both situations there is a large savings in the time and expense of carrying out the many chemical reactions and their corresponding handling and puri cation steps.

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Insoluble polymer reagents, catalysts, and reagents have received the most attention, but there is increasing work with soluble polymer reagents, catalysts, and reagents [Bergbreiter, 2001, 2002; Osburn and Bergbreiter, 2001; Toy and Janda, 2000] Insoluble functional polymers have some de ciencies They are dif cult to characterize and monitoring of the progress of reaction is also dif cult Insoluble functional polymers often show low reactivity and altered selectivity (chemo-, regio-, and stereoselectivity compared to the corresponding small-molecule reactions) Soluble reagents, catalysts, and reagents are easy to characterize, and their chemical behavior is much closer to that of the small-molecule reactions This makes it easier to make the transition from small-molecule reactions to using soluble polymer reagents, catalysts, and reagents Poly(ethylene glycol) (PEG) is extensively used as a soluble polymer support It is a low molecular weight poly(ethylene oxide) with hydroxyl groups at both chain ends.

The terminal hydoxyl groups allow for attachment of a wide range of other functional groups that.

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vb.net itextsharp merge pdf files

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vb.net code to merge pdf files

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vb.net code to merge pdf files

vb.net code to merge pdf files

vb.net itextsharp merge pdf files